CN 41-1243/TG ISSN 1006-852X
CN
Advanced Search+
Volume 44 Issue 4
Sep.  2024
Turn off MathJax
Article Contents
Article Navigation >  Diamond & Abrasives Engineering  > 2024  >  44(4): 433-439
LIU Li, SHAO Fangyuan, LUO Yucai, WU Qiang, YU Jiantao, YU Jinping, WANG Haikuo, HOU Zhiqiang, WANG Chao, YANG Yikan. Pressure-transmitting properties of pyrophyllites from different localities[J]. Diamond & Abrasives Engineering, 2024, 44(4): 433-439. doi: 10.13394/j.cnki.jgszz.2023.0152
Citation: LIU Li, SHAO Fangyuan, LUO Yucai, WU Qiang, YU Jiantao, YU Jinping, WANG Haikuo, HOU Zhiqiang, WANG Chao, YANG Yikan. Pressure-transmitting properties of pyrophyllites from different localities[J]. Diamond & Abrasives Engineering, 2024, 44(4): 433-439. doi: 10.13394/j.cnki.jgszz.2023.0152
shu

Pressure-transmitting properties of pyrophyllites from different localities

doi: 10.13394/j.cnki.jgszz.2023.0152
  • 1.

    CNPC Engineering Technology R & D Company Limited, Beijing 102206, China

  • 2.

    PetroChina Huabei Oilfield Company, Renqiu 062552, Hebei, China

  • 3.

    College of Energy Engineering, Zhejiang University, Hangzhou 310027, China

More Information
  • Received Date: 2023-07-29
  • Accepted Date: 2023-11-20
  • Rev Recd Date: 2023-10-30
    • Available Online: 2024-09-25
    Abstract
  •   Objectives  Pyrophyllite, as a sealed pressure medium, has been widely used in high-pressure research for laboratories and industrial synthesis. A highly efficient pressure transfer medium can generate higher cell pressure at the same loading force. The use of a highly efficient pressure transfer medium reduces the risk of anvil rupture and production costs. Therefore, it is important to develop a suitable and efficient pressure-transmitting pyrophyllite.  Methods  The pressure calibration of four pyrophyllites from different localities at room temperature was conducted in a 6 × 8 MN multi-anvil large-volume press. The relationship between loading force and cell pressure at room temperature was established. The influence of mineral composition changes in pyrophyllite on pressure-transmitting efficiency was studied using X-ray diffraction.  Results  By investigating the influence of mineral composition changes in pyrophyllite on pressure-transmitting efficiency, the results are as follows: (1) When achieving the same cell pressure, the required loading force for Pyrophyllite 4 is 10% lower than those for the other three pyrophyllites, indicating that Pyrophyllite 4 has the best pressure-transmitting efficiency. (2) As cell pressure increases, the relationship between cell pressure and loading force begins to deviate from linearity, and the pressure-transmitting efficiency of pyrophyllite gradually decreases. When the cell pressure exceeds 5.00 GPa, applying higher loading force does not significantly increase the cell pressure. (3) Higher hardness minerals (such as Diaspore, Boehmite) in pyrophyllite can effectively improve pressure-transmitting efficiency in the low-pressure stage (cell pressure 2.55-3.68 GPa). When the minerals in pyrophyllite undergo phase transformation to form new minerals with higher hardness (such as Muscovite and Kaolinite) in the high-pressure stage (cell pressure of 5.50 GPa), pressure-transmitting efficiency can be effectively improved.  Conclusions  Pyrophyllite 4 has better pressure-transmitting efficiency than Pyrophyllite 2 does in the high-pressure stage, but it is prone to failure in sealing due to the changes in mineral composition. However, Pyrophyllite 2 shows good elastic recovery effect and sealing performance and can stably complete compression and decompression work. Considering both pressure-transmitting efficiency and sealing effect, Pyrophyllite 2 has better application value and economic benefits.

     

    • FullText(HTML)
  • loading
    • References(26)
  • [1]
    YUAN Y F, ZHU X D, ZHOU Y H, et al. Pressure-engineered optical properties and emergent superconductivity in chalcopyrite semiconductor ZnSiP2 [J]. NPG Asia Materials,2021,13(1):15. doi: 10.1038/s41427-021-00285-0
    [2]
    YAMANE R, KOMATSU K, GOUCHI J, et al. Experimental evidence for the existence of a second partially-ordered phase of ice VI [J]. Nature Communications,2021,12(1):1129. doi: 10.1038/s41467-021-21351-9
    [3]
    BIESNER T, LI W, TSIRLIN A A, et al. Spectroscopic trace of the Lifshitz transition and multivalley activation in thermoelectric SnSe under high pressure [J]. NPG Asia Materials,2021,13(1):12. doi: 10.1038/s41427-021-00283-2
    [4]
    ZHANG J W, HE D W, FANG L M, et al. The effect of size matching between anvils and the pressure transmitting medium on the pressure-generation efficiency and sealing performance for a large volume cubic pressure cell [J]. Review of Scientific Instruments,2020,91(12):125103. doi: 10.1063/5.0018188
    [5]
    FANG L M, HE D W, CHEN C, et al. Effect of precompression on pressure-transmitting efficiency of pyrophyllite gaskets [J]. High Pressure Research,2007,27(3):367-374. doi: 10.1080/08957950701553796
    [6]
    WANG H K, HE D W, TAN N, et al. Note: An anvil-preformed gasket system to extend the pressure range for large volume cubic presses [J]. Review of Scientific Instruments,2010,81(11):116102. doi: 10.1063/1.3488606
    [7]
    WU J J, LIU F M, ZHANG J W, et al. Cobalt-doped magnesium oxide pressure-transmitting medium for high pressure and high-temperature apparatus [J]. High Pressure Research,2018,38(4):448-457. doi: 10.1080/08957959.2018.1510922
    [8]
    ZHANG S Y, ZHANG H F. Genesis of the Baiyun pyrophyllite deposit in the central Taihang Mountain, China: Implications for gold mineralization in wall rocks [J]. Ore Geology Reviews,2020,120:103313. doi: 10.1016/j.oregeorev.2020.103313
    [9]
    BERGAYA F, LAGALY G. Handbook of clay science [M]. Amsterdam: Elsevier Science Ltd, 2013.
    [10]
    BENTAYEB A, AMOURIC M, OLIVES J, et al. XRD and HRTEM characterization of pyrophyllite from Morocco and its possible applications [J]. Applied Clay Science,2003,22(5):211-221. doi: 10.1016/S0169-1317(03)00066-8
    [11]
    GATTA G D, LOTTI P, MERLINI M, et al. Elastic behaviour and phase stability of pyrophyllite and talc at high pressure and temperature [J]. Physics and Chemistry of Minerals,2015,42:309-318. doi: 10.1007/s00269-014-0721-x
    [12]
    QIN X Z, ZHAO J, WANG J M, et al. Atomic structure, electronic and mechanical properties of pyrophyllite under pressure: A first-principles study [J]. Minerals,2020,10(9):778. doi: 10.3390/min10090778
    [13]
    MIDLANDS W. Focus on pigments [J]. Asian Chemical News,2004,10(438):22.
    [14]
    SHATSKIY A, LITASOV K D, TERASAKI H, et al. Performance of semi-sintered ceramics as pressure-transmitting media up to 30 GPa [J]. High Pressure Research,2010,30(3):443-450. doi: 10.1080/08957959.2010.515079
    [15]
    王海阔, 任瑛, 贺端威, 等. 六面顶压机立方压腔内压强的定量测量及受力分析 [J]. 物理学报,2017,66(9):090702. doi: 10.7498/aps.66.090702

    WANG Haikuo, REN Ying, HE Duanwei, et al. Force analysis and pressure quantitative measurement for the high pressure cubic cell [J]. Acta Physica Sinica,2017,66(9):090702. doi: 10.7498/aps.66.090702
    [16]
    BRIDGMAN P W. The resistance of 72 elements, alloys and compounds to 100, 000 kg/cm2 [J]. Proceedings of the American Academyof Arts dnd Sciences, 1952,81(4):165,167-251.
    [17]
    HAN Q G, MA H G, ZHOU L, et al. Finite element design of double bevel anvils of large volume cubic high pressure apparatus [J]. Review of Scientific Instruments,2007,78(11):113906. doi: 10.1063/1.2814027
    [18]
    HOU Z Q, WANG H K, YANG Y N, et al. High-pressure synthesis of high-performance submicron-sized polycrystalline β-Si3N4 bulk without additives [J]. Ceramics International,2020,46(8):12449-12457. doi: 10.1016/j.ceramint.2020.02.007
    [19]
    WANG S M, HE D W, WANG W D, et al. Pressure calibration for the cubic press by differential thermal analysis and the high-pressure fusion curve of aluminum [J]. High Pressure Research,2009,29(4):806-814. doi: 10.1080/08957950903335521
    [20]
    ZHANG J W, LIU F M, WU J J, et al. Experimental study on the pressure-generation efficiency and pressure-seal mechanism for large volume cubic press [J]. Review of Scientific Instruments,2018,89(7):075106. doi: 10.1063/1.5030092
    [21]
    KAWAZOE T, NISHIYAMA N, NISHIHARA Y, et al. Pressure generation to 25 GPa using a cubic anvil apparatus with a multi-anvil 6-6 assembly [J]. High Pressure Research,2010,30(1):167-174. doi: 10.1080/08957950903503912
    [22]
    WANG H K, HE D W, YAN X Z, et al. Quantitative measurements of pressure gradients for the pyrophyllite and magnesium oxide pressure-transmitting mediums to 8 GPa in a large-volume cubic cell [J]. High Pressure Research,2011,31(4):581-591. doi: 10.1080/08957959.2011.614238
    [23]
    DECKER D L, BASSETT W A, MERRILL L, et al. High‐pressure calibration: A critical review [J]. Journal of Physical and Chemical Reference Data,1972,1(3):773-836. doi: 10.1063/1.3253105
    [24]
    何寿安, 李家璘, 成向荣, 等. 静态超高压高温技术的若干问题 [J]. 物理学报,1977,26(2):100-114. doi: 10.3321/j.issn:1000-3290.1977.02.002

    HE Shouan, LI Jialin, CHENG Xiangrong, et al. Some aspects in high pressure high temperature technology [J]. Acta Physica Sinica,1977,26(2):100-114. doi: 10.3321/j.issn:1000-3290.1977.02.002
    [25]
    FROST D J, POE B T, TRøNNES R G, et al. A new large-volume multi- anvil system [J]. Physics of the Earth and Planetary Interiors,2004,143:507-514. doi: 10.1016/j.pepi.2004.03.003
    [26]
    王海阔, 贺端威, 许超, 等. 基于国产铰链式六面顶压机的大腔体静高压技术研究进展 [J]. 高压物理学报,2013,27(5):633-661. doi: 10.11858/gywlxb.2013.05.001

    WANG Haikuo, HE Duanwei, XU Chao, et al. Development of large volume-high static pressure techniques based on the hinge-type cubic presses [J]. Chinese Journal of High Pressure Physics,2013,27(5):633-661. doi: 10.11858/gywlxb.2013.05.001
    • Relative Articles
    • Supplements(0)
    • Cited By
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(5)  / Tables(2)

    Get Citation
    PDF
    XML

    Article Metrics

    Article views (124) PDF downloads(15) Cited by()
    Proportional views
    Related
    Website Copyright © Zhengzhou Research Institute for Abrasives and Grinding Co., Ltd.  豫ICP备05008669号
    Address：No. 121, Wutong Street, Hitech Zone, Zhengzhou  Postal Code：450001
    Phone: 0371-67650914 67661785
    Email Alerts RSS

    Supported by: Beijing Renhe Information Technology Co., Ltd.    

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return